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I have a reaction chamber where gasses are injected to maintain a certain mixture. The container is sort of like a bell, where the bottom is submerged in water to make a seal.

The issue I have is that when injecting new gas into the chamber the excess has nowhere to go, so the water level is forced downward. I would like to maintain the water level difference inside and outside the chamber of <0.1in.

This rules out most kinds of check valves, because the pressure differential is too low. What I'm currently doing, is intentionally leaving a small hole open in the reaction chamber to allow pressure to equalize. Gas is injected at a very slow rate, so this works ok, but unwanted diffusion is always occurring through the hole.

Does anyone know of a mechanism that will allow the pressure to equalize, but which will not allow significant gas exchange once the pressure is equal? I'm thinking something similar to a water trap, but with even lower pressure drop.

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  • $\begingroup$ raise or lower the bell to compensate for the amount to be added. $\endgroup$ – Solar Mike May 16 '19 at 19:12
  • $\begingroup$ Are you trying to keep the pressure constant, or running this in a shallow pan so you can't move the bell, or what? How about a valve, either hand- or automatically actuated, that opens when the water level differential gets too high? $\endgroup$ – TimWescott May 16 '19 at 19:14
  • $\begingroup$ @TimWescott: Yes, both of those things. I am essentially trying to maintain atmospheric pressure in a "closed" space, into which I need to inject gasses. A valve is an interesting idea, but it would have to be a powered ball valve, since a solenoid would not operate well with such a low pressure differential. I'm hoping for a small passive device, but that's one option. $\endgroup$ – Drew May 16 '19 at 21:48
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    $\begingroup$ Your problem is that any passive device will have to be powered by the pressure differential between your dome and the outside. What's the pressure differential needed by your water trap compared to ordinary fluctuations in barometric pressure in your lab? $\endgroup$ – TimWescott May 16 '19 at 23:18
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There are specialty sensors and relays that are sensitive enough for the range of pressure you need, but they may be expensive.

one way is to hang the container in balance with a ballast weight to a gas valve like a flush mechanism.

I did a sketch which is basically you container hung in balance with a submerged Wider flange to take in more volume with little change in pressure and higher leverage, to control a small gas valve.

gas flush valve mechanism

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  • $\begingroup$ Interesting idea, thank you! $\endgroup$ – Drew May 18 '19 at 16:55

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